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Geranioksi Sübstitüentli Mononükleer Metalli Ftalosiyaninlerin Sentezi ve Karakterizasyonu
2013
Journal:  
Adıyaman University Journal of Educational Sciences
Author:  
Abstract:

Yeni disübstitüe ftalonitril türevi 3 geraniol ile 4,5-dikloro-1,2-disiyano benzenin kuru DMF çözücülü ve K2CO3 bazlı ortamda aromatik halkadaki aktif klor gruplarının nükleofilik yerdeğiştirme reaksiyonuyla hazırlandı. Ftalonitrilin 3 tetramerizasyonu mononükleer metalli ftalosiyaninleri 4 ve 5 (M = Co ve Cu) sentezlendi. Sentezlenen bileşikler FT-IR, 1H-NMR ve UV/VIS spektrumları ile karakterize edildi.

Keywords:

Synthesis and Characterization Of Mononuclear Metallo Phthalocyanines With Geranioxy Substituents
2013
Journal:  
Adıyaman University Journal of Educational Sciences
Author:  
Abstract:

A new disubstituted phthalonitrile derivative 3 was prepared by the reaction of 4-5-dichloro-1,2-dicyanobenzene and gereniol in dry DMF as solvent, in the presence K2CO3 as base, by nucleophilic displacement reaction of activated chloride groups in an aromatic ring. The tetramerization of compound 3 gave a mononuclear metallophthalocyanines 4 and 5 (M=Co and Cu). The synthesized compounds were characterized by FT-IR, 1H NMR and UV/VIS spectroscopic data.

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Adıyaman University Journal of Educational Sciences

Field :   Eğitim Bilimleri

Journal Type :   Uluslararası

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Article : 145
Cite : 874
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Adıyaman University Journal of Educational Sciences