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Yeni Bir Schiff Bazı Ve Geçiş Metalleri İle Oluşturdukları Komplekslerin Sentezi Ve Karakterizasyonu
2012
Journal:  
Bitlis Eren Üniversitesi Fen Bilimleri Dergisi
Author:  
Abstract:

Bu çalışmada, salisilaldehit ve 1,2-diborometan’ın kondenzesyonundan 2.2’-[etan-1,2-diilbis (oksi)] dibenzaldehid bileşiği sentezlendi. Bu bileşiğin 2-aminofenol ile reaksiyonundan yeni bir Schiff bazı ligandı (LH2) hazırlandı. Bu Schiff bazı ligandı ile Co+2, Ni+2 ve Zn+2 asetat tuzları reaksiyona sokularak Co(L)(H2O)2, Ni(L)(H2O)2 ve Zn(L)(H2O)2 kompleksleri elde edildi. Schiff bazı ve komplekslerinin yapıları, elementel analiz, IR, 1H-NMR, 13C-NMR, UV, manyetik duyarlılık ve termogravimetrik analiz ile aydınlatıldı.

Keywords:

Synthesis and characterization of the complexes they create with a new Schiff and transitional metals
2012
Journal:  
Bitlis Eren Üniversitesi Fen Bilimleri Dergisi
Author:  
Abstract:

In this study, the 2.2-'-[etan-1.2-diylbis (oxy)] dibenzaldehyd compound was synthesized from the condensation of salisilaldehyd and 1.2-diboromethan. A new Schiff from the reaction of this compound with 2-aminofenol (LH2) was prepared. With this Schiff some ligand, the Co+2, Ni+2 and Zn+2 acetate salts were reacted and the Co(L)(H2O)2, Ni(L)(H2O)2 and Zn(L)(H2O)2 complexes were obtained. Schiff's some and complex structures were illuminated by elementary analysis, IR, 1H-NMR, 13C-NMR, UV, magnetic sensitivity and thermogravimetric analysis.

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Bitlis Eren Üniversitesi Fen Bilimleri Dergisi

Field :   Fen Bilimleri ve Matematik; Mühendislik

Journal Type :   Ulusal

Metrics
Article : 948
Cite : 1.900
2023 Impact : 0.228
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Bitlis Eren Üniversitesi Fen Bilimleri Dergisi