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Synthesis and 3D crystal structure of new Ni(II)-ion-pair complex
2018
Journal:  
Balıkesir Üniversitesi Fen Bilimleri Enstitüsü Dergisi
Author:  
DOI:  
10.25092/baunfbed.411767
Abstract:

Yeni Ni(II) iyon-çifti kompleksi, [BzTPP][Ni(dto)2] [(dto)2- = ditiooksalat ve (BzTPP)+= benziltrifenilfosfonyum] sentezlendi ve tek kristal X-ışını kırınımı yöntemi ile karakterize edildi. Kristal yapı analizi kompleksin monoklinik uzay grubu P21/c 'de kristallendiğini ve asimetrik biriminde birbirinden ayrık olarak [BzTPP]+ organik katyonu ve [Ni(dto)2]2- kompleks anyonun yarısından oluştuğunu göstermektedir. Nikel atomu dört koordinatlıdır ve kare düzlem koordinasyon geometrisine sahiptir. Kristal yapıda, organik katyonlar ve inorganik anyonlar moleküller arası C–H···O hidrojen bağlarıyla ve C–H···π ve π−π etkileşimleriyle birbirlerine bağlanırlar, buda üç boyutlu kristal yapının oluşmasını ve kafes yapının kararlılığını sağlar.

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Balıkesir Üniversitesi Fen Bilimleri Enstitüsü Dergisi

Field :   Eğitim Bilimleri; Fen Bilimleri ve Matematik; Mühendislik

Journal Type :   Ulusal

Metrics
Article : 874
Cite : 2.467
2023 Impact : 0.115
Details
Balıkesir Üniversitesi Fen Bilimleri Enstitüsü Dergisi