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Bu çalışmada Enez (Ainos) Kazısı Su Terazisi ve Kral Kızı bölgelerinden ele geçen 19 adet etütlük cam buluntunun kimyasal içeriğinin belirlenmesi ve kimyasal içeriklerinin örneklerde görülen bozulma tabakaları ile ilişkilendirilmesi için arkeometrik incelemeler yapılmıştır. Cam buluntuların öncelikle fiziksel durumları incelenmiş, cam yüzeyinde bulunan bozulma tabakaları fotoğrafla belgelenmiş, dijital kalınlık ölçer ile kalınlıkları ölçülmüş, renk ölçümleri yapılmış ve optik mikroskop altında habbe ve bozulma ürünlerinin görüntüleri çekilerek belgelenmiştir. Roma Dönemi’ne ait etütlük örneklerin bozulma tabakaları görsel olarak ve optik mikroskop ile incelendiğinde sedef oluşumu, matlaşma, siyah kabuk oluşumu ve çukur oluşumu gibi camın kimyasal bileşiminden kaynaklanan bozulma türleri tespit edilmiştir. Camın yüzeyinde mevcut olan bozulmalar derecelendirilerek bir tablo oluşturulmuştur. Cam örneklerin bozulma tabakalarını, element ve mineralojik içeriklerini belirlemek için Mikro-XRF, Polarize Enerji Dağılımlı X-Işını Floresans (Polarized Energy Dispersive-PED-XRF), Taramalı Elektron Mikroskobu- Enerji Dağılımlı Spektrometresi (Scanning Electron Microscope-Energy Dispersive Spectrometry, SEM-EDS) ve Raman (Konfokal) Spektroskopi yöntemleri kullanılmıştır. Tüm arkeometrik sonuçlar değerlendirildiğinde, bulk cam ve bozulma tabakaları arasında farklılık olduğu ortaya koyulmuştur.
In this study, archaeometric examinations were conducted to determine the chemical content of the 19 stainless glass foundations covered from the Enez (Ainos) Water Tree and King's Daughter regions and to link the chemical content to the degradation layers seen in the samples. Glass findings first studied the physical conditions, the layers of deterioration on the glass surface were documented by photo, the thickness was measured by digital thickness measurements, the color measurements were made and the images of the defect and deterioration products were documented under the optical microscope. When the disturbance layers of the examples of the Roman era were studied visually and with an optical microscope, the disturbance types caused by the chemical composition of the glass, such as the formation of seafood, mattration, formation of black cortex and formation of holes were identified. A picture is created by classifying the disturbances present on the surface of the window. Micro-XRF, Polarized Energy Dispersive-PED-XRF, Scanning Electron Microscope-Energy Dispersive Spectrometry (SEM-EDS) and Raman (Confocal) Spectroscopy methods have been used to determine the deformation layers, element and mineral content of glass samples. When all archaeometric results were evaluated, it was found that there was a difference between bulk glass and degradation layers.
Archaeometric investigations were carried out to determine and correlate the chemical contents with the layers of deterioration of the 19 glass finds dating to the Roman Period uncovered from Su Terazisi and Kral Kızı Regions of Enez (Ainos) ancient city. The physical condition of glass finds was firstly examined, the layers of deterioration on the glass surface were documented with photographs, their thickness was measured with a digital thickness meter, their colors were identified by a chromameter, and images of the bubbles and deterioration products were taken under an optical microscope. When the deterioration layers of the samples belonging to the Roman Period were examined visually and with an optical microscope, the types of deterioration resulting from the chemical composition of the glass, such as iridescence, dulling, black discoloration and pitting were identified. A table was created of the existing degree of deterioration. Micro-XRF and Polarized Energy Dispersive-X-Ray Fluorescence (PED-XRF), Scanning Electron Microscope-Energy Dispersive Spectrometry (SEM-EDS), and Raman (Confocal) Spectroscopy methods were used to determine the element and mineralogical contents, and the deterioration layer of the glass samples. When all the archaeometric results were evaluated, it was revealed that there was a difference between the bulk glass and the deterioration layers.
Field : Güzel Sanatlar; Mimarlık, Planlama ve Tasarım
Journal Type : Ulusal
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